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- Method: HPLC analysis was performed to detect the contents of hesperidin, naringin and synephrine. 方法:HPLC測定黃酮類(lèi)成分橙皮苷和柚皮苷含量、生物堿類(lèi)辛弗林含量,藥典法測定揮發(fā)油含量。
- Methods The TLC methods were established for identified of hesperidin,synephrine and caulis perillae,and a RP-HPLC methed was established for the determination of naringin. 方法增加TLC法鑒別橙皮苷、辛弗林、紫蘇梗及RP-HPLC法測定柚皮苷含量的陰性干擾試驗。
- Methods The contents of synephrine, volatile oil, total ash, acid-insoluble ash and water in different specifications of Frutus Aurantii Immaturus were determined by HPLC or other methods according the china pharmacopoeia. 方法采用HPLC法測定不同規格枳實(shí)中辛弗林含量，同時(shí)依照藥典方法分別測定了其揮發(fā)油、總灰分、酸不溶性灰分和水分含量，對不同規格枳實(shí)藥材進(jìn)行綜合質(zhì)量對比研究，并與其傳統規格分類(lèi)進(jìn)行比較。
- To extract synephrine, the percolation processes was selected, the extraction steps include wetting powdery FAI, dipping the wet powder in hydrochloric acid solution and percolating by using hydrochloric acid solution. 通過(guò)比較選擇滲漉法提取辛弗林,提取步驟為:枳實(shí)粗粉潤濕,酸液浸泡,裝滲漉筒以鹽酸溶液滲漉。
- Evaluate the method from the following aspect: limit of detection, linearity, accuracy, stability, reproducibility and recovery rate, and determine the content of synephrine for further use. 從檢出限、線(xiàn)性關(guān)系、精密性、穩定性、重現性以及加標回收率等方面對測定方法進(jìn)行評價(jià)，并進(jìn)一步測定受試枳實(shí)提取物中辛弗林的含量備用。
- This article made a mini review of synephrine on the extraction methods,purification methods by ion-exchange and macroporous resin adsorption and determination methods by HPLC and GC-MS of synephrine. 總結了辛弗林的提取方法,離子交換樹(shù)脂、大孔吸附樹(shù)脂純化方法,高效液相色譜法、氣相色譜-質(zhì)譜聯(lián)用法測定。
- Methods The rhubarb and synephrine were dentified with TLC; 方法采用TLC法鑒別大黃、辛弗林；
- Keywords Fructus Aurantii;Naringin;Synephrine;Genuine crude drug; 機殼;柚皮甙;辛弗林;道地藥材;
- Keywords hesperdin;synephrine;gastric smooth muscle cells; 橙皮苷;辛弗林;胃平滑肌細胞;
- Keywords Capillary electrophoresis;Trifoliate orange;Synephrine;Naringenin; 毛細管電泳;枳殼;辛弗林;柚皮素;
- Keywords orthogonal test;citrus aurantium;synephrine;extracting process; 正交試驗;枳實(shí);辛弗林;提取工藝;
- Keywords Reversed phase ion-pair HPLC;Citrus aurantium L.;Synephrine;Content; 反相離子對高效液相色譜法;枳實(shí);辛弗林;含量;
- Keywords Yanyan buccal tablets;Synephrine;HPLC;Content determination; 咽炎口含片;辛弗林;高效液相色譜法;含量測定;
- sympatol 交感酚
- Keywords supercritical fluid chromatography;packed-Column;Fructus Aurantii Immaturus;synephrine; 超臨界流體色譜;填充柱;枳實(shí);辛弗林;
- oxedrine 羥基去甲麻黃素, 對羥福林
- Keywords Synephrine;Fructus Aurantii Immaturus;Extract;Ion-exchange;Process optimization; 枳實(shí);辛弗林;滲漉;離子交換;工藝優(yōu)化;
- Oxedrine measurement 羥基去甲麻黃素測量
- Keywords Jiuxin Fumai Injection;Synephrine;N-methyltyramine;Citrus anrantium L;Rat;Long-term toxicity; 救心復脈注射液;對羥福林;N-甲基酪胺;枳實(shí);大鼠;長(cháng)期毒性;
- oxedrine tartrate 酒石酸對羥福林
