Z =8. The X-ray diffraction intensity data were collected on a four-circle diffractometer. The strueture has been solved by direct method and refined by block-diagonal least squares method. The final R wag 0.075 for 3146 independent observed reflexions.
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- Z=8.；用四圓衍射儀收集X射線(xiàn)衍射強度數據；用直接法解晶體結構；用塊對角矩陣最小二乘法進(jìn)行結構修正；參與修正的可觀(guān)測獨立反射點(diǎn)共3146個(gè)
